Technology Services, Weights and Measures Division, NIST

NIST Handbook 143
State Weights and Measures Laboratories Program Handbook

7. Specific Technical Guidelines

The following information is primarily from the NVLAP Calibration Laboratories Technical Guide, and is used here as the technical guidelines for evaluation of traceability resulting in the issuance of a Certificate of Traceability.

"This section provides examples and guidelines, not requirements, to technical experts and interested calibration laboratories, on good laboratory practices and recommended standards. Therefore, the guide language reflects this philosophy through the use of "shoulds" instead of "shalls" (along with other less prescriptive language) when describing criteria. Absolute requirements are not presented here since they depend on the measurement uncertainty for which an applicant laboratory wishes to be accredited. This is a business decision for each laboratory and beyond the scope of this voluntary program. Simply stated, to be [recognized or] accredited an applicant laboratory must have a quality system and be able to prove (and document) that it does what it says it does (i.e., correctly calibrate to a stated uncertainty).

This guide is dynamic in that new parameters may be added and existing criteria updated and improved."

Recognition Parameter Summary

Each laboratory must specify the range and uncertainty level for each parameter for which it requests recognition. Uncertainties must be defined at each level. For example, a chart must be available that will state each nominal mass, each nominal volume, and so on, with the associated uncertainty.

 

Table 3. Recognition parameter summary

Parameter
Range/Application
Expanded Uncertainty
Mass
laboratory to detail nominal ranges and uncertainties: e.g., 30 kg to 1 mg; Echelon II
Echelon I ASTM Class 1, 1.1, OIML Class E1, E2 0.25 mg at 1 kg, and 1 to 5 mg/kg 
Echelon II ASTM Class 2, 3, OIML Class F1, F2 1 mg/kg to 20 mg/kg
Echelon III ASTM Class 4, 5, 6, OIML Class M1, M2, M3

NIST Class F, legal/regulatory enforcement

20 mg/kg to 1 000 mg/kg
Length
laboratory to specify range: e.g., 10 cm to 20 meter tapes
Tapes, bench method up to 25 m (100 ft) 0.0 001 m to 0.000 14 m
Tapes, tape method up to 25 m (100 ft) 0.000 15 m to 0.000 25 m
Rules, direct comparison up to 0.5 cm (18 in) < 0.000 05 m
Volume
laboratory to specify ranges: e.g., 2 ?Liter micropipettes to 2000 mL glass flasks
Gravimetric syringes, micropipettes, glass standards, and metal provers 0.000 10 mL/L
Volume transfer glass standards and metal provers < 0.001 mL/L
Temperature
laboratory to specify type and ranges: e.g., -10 °C to 200 °C; Echelon II
Echelon I SPRT's £ ± 0.005 °C
Echelon II Thermistors, thermocouples > ± 0.005 °C to £ ± 0.05 °C
Echelon III Liquid-in-glass thermometers > ± 0.05 °C to £ ± 0.20 °C
Echelon IV Liquid-in-glass, dial type, pyrometers > ± 0.20 °C to £ ± 1.0 °C
Echelon V Infra-red sensors, thermographs > ± 1.0 °C to £ ± 5.0 °C
Tuning Forks 
as used for law enforcement 0.05 mph, estimate based on interlaboratory tests
Hydrometers
sugar, syrup, petroleum estimate
Time 
stopwatches used for law enforcement significantly less than tolerances; estimated at 2 s for a 24 hr test 
Grain Moisture
programs for testing grain and commodity moisture
Oven Methods
laboratory to specify methods and products 0.2% moisture content
Chemical Methods
0.2% moisture content

*General estimates of ranges only. Detailed uncertainties must be provided for each parameter and range.

  Additional Elements
Link
7.1

Technical Criteria for Dimensional Laboratories

7.2 Technical Criteria for Mass Laboratories
  Table 8. Summary of Mass Requirements
7.3 Technical Criteria for Volume Laboratories
  Table 12. Summary of Volume Requirements
bullet link
7.4 Technical Criteria for Hydrometer Laboratories
7.5 Technical Criteria for Thermometer Laboratories
7.6 Technical Criteria for Moisture Laboratories
  Table 14. Summary of Environmental Facility Guidelines
 

Created: December 4, 2002
Last Update: February 15, 2006
Your comments and suggestions are solicited: owm@nist.gov



 

 


 

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