NIST Handbook 143 State Weights and Measures Laboratories Program Handbook | | 7. Specific Technical Guidelines The following information is primarily from the NVLAP Calibration Laboratories Technical Guide, and is used here as the technical guidelines for evaluation of traceability resulting in the issuance of a Certificate of Traceability. "This section provides examples and guidelines, not requirements, to technical experts and interested calibration laboratories, on good laboratory practices and recommended standards. Therefore, the guide language reflects this philosophy through the use of "shoulds" instead of "shalls" (along with other less prescriptive language) when describing criteria. Absolute requirements are not presented here since they depend on the measurement uncertainty for which an applicant laboratory wishes to be accredited. This is a business decision for each laboratory and beyond the scope of this voluntary program. Simply stated, to be [recognized or] accredited an applicant laboratory must have a quality system and be able to prove (and document) that it does what it says it does (i.e., correctly calibrate to a stated uncertainty). This guide is dynamic in that new parameters may be added and existing criteria updated and improved." Recognition Parameter Summary Each laboratory must specify the range and uncertainty level for each parameter for which it requests recognition. Uncertainties must be defined at each level. For example, a chart must be available that will state each nominal mass, each nominal volume, and so on, with the associated uncertainty. | | Table 3. Recognition parameter summary | Parameter | Range/Application | Expanded Uncertainty | | Mass | laboratory to detail nominal ranges and uncertainties: e.g., 30 kg to 1 mg; Echelon II | | Echelon I | ASTM Class 1, 1.1, OIML Class E1, E2 | 0.25 mg at 1 kg, and 1 to 5 mg/kg | | Echelon II | ASTM Class 2, 3, OIML Class F1, F2 | 1 mg/kg to 20 mg/kg | | Echelon III | ASTM Class 4, 5, 6, OIML Class M1, M2, M3 NIST Class F, legal/regulatory enforcement | 20 mg/kg to 1 000 mg/kg | | Length | laboratory to specify range: e.g., 10 cm to 20 meter tapes | | Tapes, bench method | up to 25 m (100 ft) | 0.0 001 m to 0.000 14 m | | Tapes, tape method | up to 25 m (100 ft) | 0.000 15 m to 0.000 25 m | | Rules, direct comparison | up to 0.5 cm (18 in) | < 0.000 05 m | | Volume | laboratory to specify ranges: e.g., 2 ?Liter micropipettes to 2000 mL glass flasks | | Gravimetric | syringes, micropipettes, glass standards, and metal provers | 0.000 10 mL/L | | Volume transfer | glass standards and metal provers | < 0.001 mL/L | | Temperature | laboratory to specify type and ranges: e.g., -10 °C to 200 °C; Echelon II | | Echelon I | SPRT's | £ ± 0.005 °C | | Echelon II | Thermistors, thermocouples | > ± 0.005 °C to £ ± 0.05 °C | | Echelon III | Liquid-in-glass thermometers | > ± 0.05 °C to £ ± 0.20 °C | | Echelon IV | Liquid-in-glass, dial type, pyrometers | > ± 0.20 °C to £ ± 1.0 °C | | Echelon V | Infra-red sensors, thermographs | > ± 1.0 °C to £ ± 5.0 °C | | Tuning Forks | as used for law enforcement | 0.05 mph, estimate based on interlaboratory tests | | Hydrometers | sugar, syrup, petroleum | estimate | | Time | stopwatches used for law enforcement | significantly less than tolerances; estimated at 2 s for a 24 hr test | | Grain Moisture | programs for testing grain and commodity moisture | | Oven Methods | laboratory to specify methods and products | 0.2% moisture content | | Chemical Methods | 0.2% moisture content | *General estimates of ranges only. Detailed uncertainties must be provided for each parameter and range. | | | Additional Elements | Link | | 7.1 | Technical Criteria for Dimensional Laboratories | | | 7.2 | Technical Criteria for Mass Laboratories | | | | Table 8. Summary of Mass Requirements | | | 7.3 | Technical Criteria for Volume Laboratories | | | | Table 12. Summary of Volume Requirements | | | 7.4 | Technical Criteria for Hydrometer Laboratories | | | 7.5 | Technical Criteria for Thermometer Laboratories | | | 7.6 | Technical Criteria for Moisture Laboratories | | | | Table 14. Summary of Environmental Facility Guidelines | | | | | Created: December 4, 2002 Last Update: February 15, 2006 Your comments and suggestions are solicited: owm@nist.gov
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